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Highly efficient aza-Baylis-Hillman reaction of N-tosylated imines with MVK, acrolein, and phenyl acrylate or alpha-naphthyl acrylate: Lewis base effects and a convenient method to synthesize alpha,beta-unsaturated beta-amino carbonyl compounds
其他题名磺酰亚胺和丁烯酮, 丙烯醛, 丙烯酸苯酯和萘酯的高效aza-Baylis-Hillman反应: Lewis碱的效应和????不饱和 ?-氨基酮类化合物的简便合成法
Xu YM(徐永梅); Shi M(施敏); Shi M(施敏)
2004
发表期刊J. Org. Chem.
卷号69期号:2页码:417-425
摘要This paper describes several highly efficient aza-Baylis-Hillman reactions of N-tosylated imines with MVK, acrolein, and phenyl acrylate or alpha-naphthyl acrylate in the presence of a Lewis base. In most cases, the reaction can be completed within 1 h using the appropriate Lewis base catalyst. An efficient method to synthesize beta-amino ketones, aldehydes and esters in high yields and short reaction time has been developed.
学科领域金属有机化学
部门归属中国科学院上海有机化学研究所金属有机化学实验室
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收录类别SCI
语种英语
WOS记录号WOS:000188496300022
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文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/9926
专题金属有机化学国家重点实验室
通讯作者Shi M(施敏)
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GB/T 7714
Xu YM,Shi M,Shi M. Highly efficient aza-Baylis-Hillman reaction of N-tosylated imines with MVK, acrolein, and phenyl acrylate or alpha-naphthyl acrylate: Lewis base effects and a convenient method to synthesize alpha,beta-unsaturated beta-amino carbonyl compounds[J]. J. Org. Chem.,2004,69(2):417-425.
APA Xu YM,Shi M,&施敏.(2004).Highly efficient aza-Baylis-Hillman reaction of N-tosylated imines with MVK, acrolein, and phenyl acrylate or alpha-naphthyl acrylate: Lewis base effects and a convenient method to synthesize alpha,beta-unsaturated beta-amino carbonyl compounds.J. Org. Chem.,69(2),417-425.
MLA Xu YM,et al."Highly efficient aza-Baylis-Hillman reaction of N-tosylated imines with MVK, acrolein, and phenyl acrylate or alpha-naphthyl acrylate: Lewis base effects and a convenient method to synthesize alpha,beta-unsaturated beta-amino carbonyl compounds".J. Org. Chem. 69.2(2004):417-425.
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