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Study on the accelerated Gutknecht selfcyclocondensation of amino-sugars under atmospheric pressure chemical ionization conditions
Alternative Title大气压化学电离条件下氨基糖加速Gutknecht自缩合的研究
Wang HY(王昊阳)1; Zhang JT(张骏婷)1; Sun SH(孙世豪)1; Zhang SS(张曙盛)1; Zhang F(张芳)1; Zhu H(朱晖)1; Guo YL(郭寅龙)1
2015
Source PublicationRSC Adv.
Volume5Issue:127Pages:105079-105083
AbstractAn unexpected gas phase Gutknecht self-condensation of D-glucosamine hydrochloride to 2,5-deoxyfructosazine (2,5-DOF) in atmospheric pressure chemical ionization mass spectrometry (APCI-MS) was described. Mechanistic studies indicated that the thermospray conditions in APCI largely accelerate the irreversible Gutknecht self-cyclocondensation reaction of amino-sugars. Our observations provide a promising clue for a new borate-free synthetic method of 2,5-DOF by mimicking the APCI conditions.
Subtype论文
Subject Area分析化学
DOI10.1039/c5ra22331h
URL查看原文
Indexed BySCI
Language英语
WOS IDWOS:000366865900052
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Document Type期刊论文
Identifierhttp://ir.sioc.ac.cn/handle/331003/39698
Collection分析化学研究室
Corresponding AuthorWang HY(王昊阳); Guo YL(郭寅龙)
Affiliation1.中科院上海有机化学研究所
2.中国烟草总公司郑州烟草研究院
Recommended Citation
GB/T 7714
Wang HY,Zhang JT,Sun SH,et al. Study on the accelerated Gutknecht selfcyclocondensation of amino-sugars under atmospheric pressure chemical ionization conditions[J]. RSC Adv.,2015,5(127):105079-105083.
APA 王昊阳.,张骏婷.,孙世豪.,张曙盛.,张芳.,...&郭寅龙.(2015).Study on the accelerated Gutknecht selfcyclocondensation of amino-sugars under atmospheric pressure chemical ionization conditions.RSC Adv.,5(127),105079-105083.
MLA 王昊阳,et al."Study on the accelerated Gutknecht selfcyclocondensation of amino-sugars under atmospheric pressure chemical ionization conditions".RSC Adv. 5.127(2015):105079-105083.
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