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Efficient synthesis of pyrrolo[2,3-d]pyrimidines via a Cu(I)/6-methylpicolinic acid catalyzed coupling reaction
Alternative Title铜(I)/6-甲基-哌啶-2-羧酸催化的偶联反应合成吡咯并嘧啶化合物
Jiang X(蒋西)1; Sun DQ(孙德群)1; Jiang YW(蒋咏文)1; Ma DW(马大为)1
2015
Source PublicationTetrahedron Lett.
Volume56Issue:23Pages:3259-3261
AbstractCopper/6-methylpicolinic acid catalyzed coupling reaction of substituted 5-bromopyrimidin-4-amines with alkynes and subsequent cyclization took place in DMSO at 100-110 degrees C to afford 2-chloro-pyrrolo [2,3-d]pyrimidines in moderate to excellent yields. Variable functional groups, including aromatic and aliphatic groups, could be introduced at the 6 and 7 positions using this method. (C) 2014 Elsevier Ltd. All rights reserved.
Subtype论文
Subject Area生命有机化学
DOI10.1016/j.tetlet.2014.12.098
URL查看原文
Indexed BySCI
Language英语
WOS IDWOS:000356544800071
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Document Type期刊论文
Identifierhttp://ir.sioc.ac.cn/handle/331003/39511
Collection生命有机化学国家重点实验室
Corresponding AuthorJiang YW(蒋咏文); Ma DW(马大为)
Affiliation1.山东大学威海分校
2.中科院上海有机化学研究所, 生命有机化学国家重点实验室
Recommended Citation
GB/T 7714
Jiang X,Sun DQ,Jiang YW,et al. Efficient synthesis of pyrrolo[2,3-d]pyrimidines via a Cu(I)/6-methylpicolinic acid catalyzed coupling reaction[J]. Tetrahedron Lett.,2015,56(23):3259-3261.
APA 蒋西,孙德群,蒋咏文,&马大为.(2015).Efficient synthesis of pyrrolo[2,3-d]pyrimidines via a Cu(I)/6-methylpicolinic acid catalyzed coupling reaction.Tetrahedron Lett.,56(23),3259-3261.
MLA 蒋西,et al."Efficient synthesis of pyrrolo[2,3-d]pyrimidines via a Cu(I)/6-methylpicolinic acid catalyzed coupling reaction".Tetrahedron Lett. 56.23(2015):3259-3261.
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