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学科主题: 有机化学
题名: One-pot synthesis of trifluoromethylated phthalans via intramolecular cyclization from 2-alkynylbenzaldehydes
其他题名: 2-炔基芳醛的分子内环化"一锅法"合成三氟甲基苯并呋喃
作者: Xu LJ(徐利军)1; Jiang HZ(蒋海珍)1; Hao J(郝健)1; Zhao G(赵刚)1
通讯作者: 蒋海珍 ; 郝健 ; 赵刚
刊名: Tetrahedron
发表日期: 2014
DOI: 10.1016/j.tet.2014.04.072
卷: 70, 期:29, 页:4373-4378
收录类别: SCI
英文摘要: An efficient tandem addition/cyclization procedure for the synthesis of trifluoromethylated phthalans under mild conditions was developed. This procedure involves tetrabutylammonium fluoride (TBAF)-promoted addition of Ruppert-Prakash reagent (TMSCF3) to 2-alkynylbenzaldehyde to give 2-alkynylbenzylicalcohols, which would then undergo base-catalyzed selective 5-exo-dig cyclization to furnish the corresponding products. (C) 2014 Elsevier Ltd. All rights reserved.
语种: 英语
相关网址: 查看原文
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/39163
Appears in Collections:上海有机化学研究所_期刊论文

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作者单位: 1.上海大学
2.中科院上海有机化学研究所

Recommended Citation:
Xu LJ,Jiang HZ,Hao J,et al. One-pot synthesis of trifluoromethylated phthalans via intramolecular cyclization from 2-alkynylbenzaldehydes[J]. Tetrahedron,2014,70(29):4373-4378.
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