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Fluorinated graphene: facile solution preparation and tailorable properties by fluorine-content tuning
其他题名氟化石墨烯: 便利的溶液合成法和氟含量对性能的调控
Zhao FG(赵福刚)1; Zhao G(赵刚)1; Liu XH(刘新华)1; Ge CW(葛从伍)1; Wang JT(王金土)1; Li BL(李柏力)1; Wang QG(王启刚)1; Li WS(李维实)1; Chen QY(陈庆云)1
2014
发表期刊J. Mater. Chem. A
卷号2期号:23页码:8782-8789
摘要Fluorinated graphene is one of the most important two-dimensional carbon nanomaterials derived from graphene, and possesses specific and outstanding properties. However, it lacks a cost-effective and large-scale preparation method. Here, we describe a novel and facile solution approach using graphene oxide (GO) and liquid diethylaminosulfur trifluoride as starting materials under mild conditions. The chemical composition and the structure of so-prepared fluorinated graphene were characterized in detail by elemental analysis, solid state F-19 NMR, XPS, FT-IR, Raman, SEM, TEM, and AFM. These studies reveal that some oxygen-containing moieties in GO are converted into C-F bonds, while some are eliminated during the reaction. More interestingly, the fluorine-loading amount can be well tuned by simply altering the reaction medium, and has a significant impact on the optical, electronic, and conductive properties of the product. Preliminary experiments on its application as an electrode material for solid-state supercapacitors were finally presented.
学科领域氟化学
DOI10.1039/c4ta00847b
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收录类别SCI
语种英语
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文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/39162
专题上海有机化学研究所
通讯作者Wang QG(王启刚); Li WS(李维实); Chen QY(陈庆云)
作者单位1.中科院上海有机化学研究所
2.同济大学
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GB/T 7714
Zhao FG,Zhao G,Liu XH,et al. Fluorinated graphene: facile solution preparation and tailorable properties by fluorine-content tuning[J]. J. Mater. Chem. A,2014,2(23):8782-8789.
APA 赵福刚.,赵刚.,刘新华.,葛从伍.,王金土.,...&陈庆云.(2014).Fluorinated graphene: facile solution preparation and tailorable properties by fluorine-content tuning.J. Mater. Chem. A,2(23),8782-8789.
MLA 赵福刚,et al."Fluorinated graphene: facile solution preparation and tailorable properties by fluorine-content tuning".J. Mater. Chem. A 2.23(2014):8782-8789.
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