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学科主题: 氟化学
题名: Synthesis and Identification of Solution-Stable Sulfenic Acids: Perfluoroalkanesulfenic Acids
其他题名: 在溶剂中稳定的新型次磺酸的合成与鉴定: 全氟烷基次磺酸
作者: Li XB(李晓波); Xu ZF(徐泽锋); Liu LJ(刘丽娟); Liu JT(刘金涛)
通讯作者: 刘金涛
刊名: Eur. J. Org. Chem.
发表日期: 2014
DOI: 10.1002/ejoc.201301563
卷: 2014, 期:6, 页:1182-1188
收录类别: SCI
英文摘要: Taking advantage of the strong electron-withdrawing effect of perfluoroalkyl groups, solution-stable perfluoroalkanesulfenic acids were synthesized for the first time by Cope-type elimination of the corresponding imines; the acids were identified by H-1 NMR, F-19 NMR, and IR spectroscopy and mass spectrometry. Trapping reagents were utilized to capture the in situ generated sulfenic acids, which provided further experimental evidence for the formation of these fluorinated sulfenic acids.
语种: 英语
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/38834
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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作者单位: 中科院上海有机化学研究所

Recommended Citation:
Li XB,Xu ZF,Liu LJ,et al. Synthesis and Identification of Solution-Stable Sulfenic Acids: Perfluoroalkanesulfenic Acids[J]. Eur. J. Org. Chem.,2014,2014(6):1182-1188.
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