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Analysis of Volatile Compounds from Siraitia grosvenorii by Headspace Solid-Phase Microextraction and Gas Chromatography-Quadrupole Time-of-Flight Mass Spectrometry
其他题名顶空固相微萃取与GC-QTOF MS联用法分析罗汉果中的挥发性成分
Xia Y(夏毅)1; Zhang F(张芳)1; Wang WY(汪维云)1; Guo YL(郭寅龙)1
2014
发表期刊J. Chromatogr. Sci.
卷号53期号:1页码:1-7
摘要Headspace solid-phase microextraction (HS–SPME) coupled with gas chromatography-quadrupole time-of-flight mass spectrometry (GC-QTOF MS) has been used in the present study to isolate and identify volatile components from Siraitia grosvenorii, a herbaceous perennial vine used as a natural sweetener and medicine. Compared with the static HS extraction and the different SPME fiber coatings, HS-SPME with divinylbenzene/carboxen/polydimethylsiloxane fiber was preferred to extract the target analytes including aldehyde, alcohol, acid, ester and other compounds. In the identification, a multi-dimensional qualitative analysis approach containing library searching, retention index comparison, accurate mass measurement, the second-stage mass spectrum (MS2 spectrum) and area normalization was utilized. Finally, a total of 46 compounds were identified from S. grosvenorii. Among them, n-hexadecanoic acid, 5-ydroxymethylfurfural, 2,3-dihydro-3,5-dihydroxy-6-methyl-4H-pyran-4-one, (Z, Z)-9,12-octadecadienoic acid and (E, E)-2,4-nonadienal were the main volatile components. The results showed that HS-SPME coupled with GC-QTOF MS is efficient for the extraction of polar volatiles from S. grosvenorii and accurate for the identification of volatile compounds in the complicated matrix.
学科领域分析化学
DOI10.1093/chromsci/bmu012
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语种英语
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文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/38593
专题分析化学研究室
通讯作者Wang WY(汪维云); Guo YL(郭寅龙)
作者单位1.金陵药业
2.安徽农业大学
3.中科院上海有机化学研究所
推荐引用方式
GB/T 7714
Xia Y,Zhang F,Wang WY,et al. Analysis of Volatile Compounds from Siraitia grosvenorii by Headspace Solid-Phase Microextraction and Gas Chromatography-Quadrupole Time-of-Flight Mass Spectrometry[J]. J. Chromatogr. Sci.,2014,53(1):1-7.
APA 夏毅,张芳,汪维云,&郭寅龙.(2014).Analysis of Volatile Compounds from Siraitia grosvenorii by Headspace Solid-Phase Microextraction and Gas Chromatography-Quadrupole Time-of-Flight Mass Spectrometry.J. Chromatogr. Sci.,53(1),1-7.
MLA 夏毅,et al."Analysis of Volatile Compounds from Siraitia grosvenorii by Headspace Solid-Phase Microextraction and Gas Chromatography-Quadrupole Time-of-Flight Mass Spectrometry".J. Chromatogr. Sci. 53.1(2014):1-7.
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