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Optically Active Monoacylglycerols: Synthesis and Assessment of Purity
其他题名光学活性甘油单酯的合成及纯度评估
Chen CY(陈超远); Han WB(韩伟博); Chen HJ(陈慧君); Wu YK(伍贻康); Gao P(高坡)
2013
发表期刊Eur. J. Org. Chem.
ISSN1434-193X
卷号2013期号:20页码:4311-4318
摘要Abstract Despite their simple structures, synthesis of 1(or 3)-acyl-sn-glycerols remains a challenge that cannot be ignored because of facile acyl migrations, which not only complicate the synthesis but also make direct GC or HP</td></tr> <tr><td class="col-xs-1 right"><strong>学科领域</strong></td><td class="col-xs-9 table-display-inline"><a href="/simple-search?query1=%E7%94%9F%E5%91%BD%E6%9C%89%E6%9C%BA%E5%8C%96%E5%AD%A6&field1=dc.subject.discipline&advanced=false">生命有机化学</a> </td></tr> <tr><td class="col-xs-1 right"><strong>部门归属</strong></td><td class="col-xs-9 table-display-inline">中国科学院上海有机化学研究所, 生命有机化学国家重点实验室 ; 黑龙江大学 </td></tr> <tr><td class="col-xs-1 right"><strong>URL</strong></td><td class="col-xs-9 table-display-inline" style="word-break:break-all;"><a target='_blank' href="http://dx.doi.org/10.1002/ejoc.201300247">查看原文</a> </td></tr> <tr><td class="col-xs-1 right"><strong>收录类别</strong></td><td class="col-xs-9 table-display-inline"><a href="/simple-search?query1=SCI&field1=dc.citation.indexedby&advanced=false">SCI</a> </td></tr> <tr><td class="col-xs-1 right"><strong>语种</strong></td><td class="col-xs-9 table-display-inline">英语 </td></tr> <tr><td class="col-xs-1 right"><strong>WOS记录号</strong></td><td class="col-xs-9 table-display-inline">WOS:000321737700018 </td></tr> <tr><td class="col-xs-1 right"><strong>引用统计</strong></td><td class="col-xs-9 table-display-inline"><div class='sci-citation-data-item'> 被引频次:<a href='http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcApp=PARTNER_APP&SrcAuth=LinksAMR&KeyUT=WOS:000321737700018&DestLinkType=CitingArticles&DestApp=ALL_WOS&UsrCustomerID=3a85505900f77cc629623c3f2907beab' title='查看引用文章' target='_blank' class='red-decoration red-border'>8</a>[WOS]   <a href='http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcApp=PARTNER_APP&SrcAuth=LinksAMR&KeyUT=WOS:000321737700018&DestLinkType=FullRecord&DestApp=ALL_WOS&UsrCustomerID=3a85505900f77cc629623c3f2907beab' target='_blank'>[WOS记录]</a>     <a href='http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcApp=PARTNER_APP&SrcAuth=LinksAMR&KeyUT=WOS:000321737700018&DestLinkType=RelatedRecords&DestApp=ALL_WOS&UsrCustomerID=3a85505900f77cc629623c3f2907beab' target='_blank'>[WOS相关记录]</a> </div> </td></tr> <tr><td class="col-xs-1 right"><strong>文献类型</strong></td><td class="col-xs-9 table-display-inline"><a class="red-decoration red-border" href="/simple-search?query1=%22%E6%9C%9F%E5%88%8A%E8%AE%BA%E6%96%87%22&field1=dc.type&advanced=false">期刊论文</a> </td></tr> <tr><td class="col-xs-1 right"><strong>条目标识符</strong></td><td class="col-xs-9 table-display-inline" style="word-break:break-all;"><a target='_blank' href='/handle/331003/29351'>http://ir.sioc.ac.cn/handle/331003/29351</a> </td></tr> <tr><td class="col-xs-1 right"><strong>专题</strong></td><td class="col-xs-9 table-display-inline"><a target='_blank' href="/handle/331003/2">生命有机化学国家重点实验室</a><br/></td></tr> </td></tr> <tr><td class="col-xs-1 right"><strong>通讯作者</strong></td><td class="col-xs-9 table-display-inline"><a href="/simple-search?query1=%E4%BC%8D%E8%B4%BB%E5%BA%B7&field1=dc.contributor.author&advanced=false">Wu YK(伍贻康)</a>; <a href="/simple-search?query1=%E9%AB%98%E5%9D%A1&field1=dc.contributor.author&advanced=false">Gao P(高坡)</a><tr><td class="col-xs-1 right"><strong>推荐引用方式</strong><br><strong>GB/T 7714</strong></td><td class="col-xs-9 table-display-inline"> Chen CY,Han WB,Chen HJ,et al. Optically Active Monoacylglycerols: Synthesis and Assessment of Purity[J]. Eur. J. Org. Chem.,2013,2013(20):4311-4318. </td></tr> <tr><td class="col-xs-1 right"><strong>APA</strong></td><td class="col-xs-9 table-display-inline"> 陈超远,韩伟博,陈慧君,伍贻康,&高坡.(2013).Optically Active Monoacylglycerols: Synthesis and Assessment of Purity.<i>Eur. J. Org. Chem.</i>,2013(20),4311-4318. </td></tr> <tr><td class="col-xs-1 right"><strong>MLA</strong></td><td class="col-xs-9 table-display-inline"> 陈超远,et al."Optically Active Monoacylglycerols: Synthesis and Assessment of Purity".<i>Eur. J. Org. 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} } var jcrfactor5=(jdata.factor5=="no results"||jdata.factor5=="")?"0":jdata.factor5; if(jcrfactor5!="0") { jcrresult+=(jcrresult=="")?jcrfactor5+"[5-Year]":","+jcrfactor5+"[5-Year]"; } if(jcrfactor!="0"||jcrfactor5!="0") { $("#tab-impact").html("(IF:"+jcrresult+")"); } else { $("#tab-impact").html(""); } } }); } else { $("#tab-impact").html(""); } } if(document.getElementById("sci-citation-data")!=null) { $("#sci-citation-data").css("color","#999"); $("#sci-citation-data").html('正在获取...'); $.get(baseURL+"/get-sci-citation", { "itemid":"509377", "num":Math.random() }, function(data) { var flag=false; if(data.length>10) { $("#sci-citation-data").css("color","#000"); var data = eval('('+data+')'); var html=""; if(data!=null) { if(data.sci_citataion[0].timesCited!=null && data.sci_citataion[0].citingArticlesURL!=null) { flag=true; html+="被引频次:<a href='"+data.sci_citataion[0].citingArticlesURL+"' title='查看引用文章' target='_blank'>"+data.sci_citataion[0].timesCited+"</a>[WOS]  "; } else if(data.sci_citataion[0].timesCited!=null && data.sci_citataion[0].timesCited=="0") { flag=true; html+="被引频次[WOS]:"+data.sci_citataion[0].timesCited+",  "; } if(data.sci_citataion[0].sourceURL!=null) { html+="<a href='"+data.sci_citataion[0].sourceURL+"' target='_blank'>[WOS记录]</a>  "; } if(data.sci_citataion[0].relatedRecordsURL!=null) { html+="<a href='"+data.sci_citataion[0].relatedRecordsURL+"' target='_blank'>[WOS相关记录]</a>"; } //html+="</div>"; } //$("#tab-sci-citation").show(); $("#sci-citation-data").html(html); } if(!flag) { $("#sci-citation-data").html("无"); $("#sci-citation-data").css("color","#999"); } }, "html"); } if(document.getElementById("cscd-citation-data")!=null) { $.get(""+"/get-cscd-citation", { item_id:509377, timeid:new Date().getTime() }, function(data){ if(data.length>10) { var data = eval('('+data+')'); $("#sci-citation-data").css("color","#000"); var html=""; if(data!=null && data.cscd_citataion[0].timesCited!=null && data.cscd_citataion[0].timesCited!="") { if(data.cscd_citataion[0].citingArticlesURL!=null) { flag=true; html+="被引频次:<a href='"+data.cscd_citataion[0].citingArticlesURL+"' title='查看引用文章' target='_blank'>"+data.cscd_citataion[0].timesCited+"</a>[CSCD]  "; } else if(data.cscd_citataion[0].timesCited=="0") { flag=true; html+="被引频次[CSCD]:"+data.cscd_citataion[0].timesCited+",  "; } if(data.cscd_citataion[0].sourceURL!=null) { html+="<a href='"+data.cscd_citataion[0].sourceURL+"' target='_blank'>[CSCD记录]</a>  "; } if(data.cscd_citataion[0].relatedRecordsURL!=null) { html+="<a href='"+data.cscd_citataion[0].relatedRecordsURL+"' target='_blank'>[CSCD相关记录]</a>"; } $("#cscd-citation-data").html(html); } else { $("#cscd-citation-data").html("无"); $("#cscd-citation-data").css("color","#999"); } //$("#tab-sci-citation").show(); } /*if(data!=null && data.citation_count!=null && data.citation_count!="-1") { //$("#tab-cscd-citation").show(); $("#cscd-citation-data").html("被引频次[CSCD]:"+data.citation_count); }*/ else { $("#cscd-citation-data").html("无"); $("#cscd-citation-data").css("color","#999"); } }, "html") } $(".pager").pager({ lang: true, pagenumber: currentPage, pagecount: pageCount, buttonClickCallback: PageClick }); $(".class-view-swf").click(function() { var id=this.id.substring(this.id.lastIndexOf("-")+1); if(id!="") { /*--var bitHandle=document.getElementById("span-view-swf-"+id); if(bitHandle!=null && bitHandle.innerHTML!="") { var swf=baseURL+"/get-swf?bitHandle="+bitHandle.innerHTML; displaySWF(swf); } else*/ { var imgLoading=document.getElementById("id-view-swf-loading-"+id); imgLoading.style.display = ""; $.get(""+"/bitstream", { orignalBitID:id, itemID:509377, method:"get-swf-bit", timeid:new Date().getTime() }, function(data){ imgLoading.style.display = "none"; if(data.substring(0,2)=="ok") { data=data.substring(3); displaySWF(baseURL+"/get-swf?bitHandle="+data); } else alert("暂不允许浏览"); }, "html") } } }); $(".class-view-video").click(function() { var id=this.id.substring(this.id.lastIndexOf("-")+1); if(id!="") { var imgHandle=document.getElementById("span-view-video-img-"+id).innerHTML; var videoHandle=document.getElementById("span-view-video-"+id).innerHTML; document.getElementById("div-video-title").innerHTML = document.getElementById("span-bit-name-"+id).innerHTML; jwplayer("myElement").setup({ width:620, height:480, file:videoHandle, image: imgHandle, primary: "flash" }); } }); setTimeout(function () { var editorone=document.getElementById("editor1"); if(editorone!=null) CKEDITOR.replace('editor1'); CKEDITOR.replace('editor2'); CKEDITOR.replace('editor3'); CKEDITOR.replace("editor4"); },500); $("#div_modify_comment").on('show.bs.modal', function(){ var $this = $(this); var $modal_dialog = $this.find('.modal-dialog'); $this.css('display', 'block'); $modal_dialog.css({'margin-top': Math.max(0, ($(window).height() - $modal_dialog.height()) / 2) }); }); }); /* function commitForm(action,obj) { $("#callURL").attr("value",window.location.href); if(action=="add") { var editor_data = CKEDITOR.instances.editor1.getData(); //var editor_data = $("#editor1").attr("value"); if(editor_data=="") { alert("请输入评论内容"); } else submitForm('add',editor_data,'0'); } else if(action=="del") { if (confirm('您确定要删除吗?')) { var id=obj.id.replace("delete_","") submitForm('delete','',id); } } }*/ function displaySWF() { var loopedSlider=document.getElementById("loopedSlider"); var viewerPlaceHolders=getElementsByClass(loopedSlider, "viewerPlaceHolder", "div"); if(viewerPlaceHolders!=null) { for(var i=0; i<viewerPlaceHolders.length; i++) { var viewerPlaceHolder = viewerPlaceHolders[i]; var swf = viewerPlaceHolder.id; //viewerPlaceHolder.style.display="block"; viewerPlaceHolder.style.width="640px"; viewerPlaceHolder.style.height="750px"; var fp = new FlexPaperViewer( ""+'/FlexPaper_1.5.1_flash/FlexPaperViewer', viewerPlaceHolder, { config : { SwfFile : swf, Scale : 0.6, ZoomTransition : 'easeOut', ZoomTime : 0.5, ZoomInterval : 0.2, FitPageOnLoad : true, FitWidthOnLoad : true, FullScreenAsMaxWindow : false, ProgressiveLoading : false, MinZoomSize : 0.2, MaxZoomSize : 5, SearchMatchAll : false, InitViewMode : 'Portrait', PrintPaperAsBitmap : false, ViewModeToolsVisible : true, ZoomToolsVisible : true, NavToolsVisible : true, CursorToolsVisible : true, SearchToolsVisible : true, localeChain: 'en_US' }}); } } } function commitCommentForm(action,obj) { if(action=="add") { var editor_data = CKEDITOR.instances.editor1.getData(); if(editor_data=="") { alert("请输入评论内容"); } else { submitAlert('loading','正在提交...'); $("#commentCurrPage").attr("value",1); $.post(baseURL+"/comment", { "type":"comment", "content":editor_data, "action":action, "resourceID":'509377', "num":Math.random() }, function(data){ if(data.substring(0,2)=="ok") submitAlert('succeed',data.substring(3)); else submitAlert('error',data); setTimeout("refreshThis();",1000); $("#item-comment").hide(); }, "html") } } else if(action=="delete") { if (confirm('您确定要删除吗?')) { var comment_id=obj.id.replace("delete_","") //submitForm('delete','',id); submitAlert('loading','正在删除...'); $("#commentCurrPage").attr("value",1); $.post(baseURL+"/comment", { "type":"comment", "commentID":comment_id, "action":action, "num":Math.random() }, function(data){ if(data.substring(0,2)=="ok") submitAlert('succeed',data.substring(3)); else submitAlert('error',data); setTimeout("refreshThis();",1000); }, "html") } } } function commitObjectionForm() { var value_editor_data = CKEDITOR.instances.editor2.getData(); var value_input_title; var value_email; var value_organization; var value_code; if(value_editor_data.trim()=="") { alert("请输入异议内容"); return; } var logined=false; if(!logined) { var input_email = document.getElementById("input-email-objection"); value_email=input_email.value.trim(); if(value_email=="") { alert("请输入Email"); return; } var input_code = document.getElementById("input-code-objection"); value_code=input_code.value; if(value_code=="") { alert("请输入验证码"); return; } var input_organization = document.getElementById("input-email-organization"); value_organization=input_organization.value.trim(); } submitAlert('loading','正在提交...'); $.post(baseURL+"/comment", { "type":"objection", "content":value_editor_data, "resourceID":'509377', "organization":value_organization, "email":value_email, "code":value_code, "num":Math.random() }, function(data) { if(dialog!=null) dialog.close(); if(data.length>3 && data.substring(0,2)=="ok") { data=data.substring(3); submitAlert('succeed',data); document.getElementById("commentFormObjection").reset(); $("#item-comment").hide(); CKEDITOR.instances.editor2.setData(""); getCaptcha(baseURL, "objection"); //setTimeout("resetForm('commentFormObjection');",3000); } else { submitAlert('error',data); } //setTimeout("refreshThis();",1000); }, "html") } function commitFeedbackForm() { var value_editor_data = CKEDITOR.instances.editor3.getData(); var value_input_title; var value_email; var value_code; var input_title = document.getElementById("input-title-feedback"); value_input_title = input_title.value.trim(); if(value_input_title=="") { alert("请填写标题"); return; } if(value_editor_data.trim()=="") { alert("请输入反馈内容"); return; } var logined=false; if(!logined) { var input_email = document.getElementById("input-email-feedback"); value_email=input_email.value.trim(); value_code=document.getElementById("input-code-objection").value; var input_code = document.getElementById("input-code-feedback"); value_code=input_code.value; if(value_code=="") { alert("请输入验证码"); return; } } submitAlert('loading','正在提交...'); $.post(baseURL+"/comment", { "type":"feedback", "content":value_editor_data, "resourceID":'509377', "title":value_input_title, "email":value_email, "code":value_code, "num":Math.random() }, function(data){ if(dialog!=null) dialog.close(); if(data.length>3 && data.substring(0,2)=="ok") { data=data.substring(3); submitAlert('succeed',data); document.getElementById("commentFormFeedback").reset(); $("#item-comment").hide(); CKEDITOR.instances.editor3.setData(""); getCaptcha(baseURL, "feedback"); //setTimeout("resetForm('commentFormObjection');",3000); } else { submitAlert('error',data); } }, "html") } function submitForm(action, comment, comment_id) { submitAlert('loading','正在提交...'); $("#commentCurrPage").attr("value",1); $.post(baseURL+"/comment", { "comment":comment, "action":action, "resourceID":'509377', "commentID":comment_id }, function(data){ submitAlert('succeed',data); setTimeout("refreshThis();",1000); }, "html") } function refreshThis() { $("#commentCurrPage").attr("value",1); $("#rndComment").attr("value",new Date().getTime()); $("#viewItemForm").submit(); } var dialog; function submitAlert(iconName, text) { dialog=art.dialog({ title:'提示', drag: false, resize: false, lock: true, background: '#ccc', // 背景色 opacity: 0.57, // 透明度 content: text, icon: iconName, ok:true }); } function resetForm(formName) { if(dialog!=null) dialog.close(); document.getElementById(formName).reset(); if(formName=="") CKEDITOR.instances.editor2.setData(""); } function alertLogin() { dialog=art.dialog({ title:'提示', drag: false, resize: false, lock: true, background: '#ccc', // 背景色 opacity: 0.57, // 透明度 content: '请您先登录!', icon: 'warning', ok:function () { window.location.href=baseURL+"/password-login"; return true; }, cancelVal: '取消', cancel: true }); } PageClick = function(pageclickednumber) { $(".pager").pager({ lang: true, pagenumber: pageclickednumber, pagecount: pageCount, buttonClickCallback: PageClick }); $("#commentCurrPage").attr("value",pageclickednumber); $("#rndComment").attr("value",new Date().getTime()); $("#viewItemForm").submit(); } function newReplay() { //var logined='false'; //if(logined=="true") //{ $("#item-comment").show(); window.location.href=window.location.href+"#new_comment"; //} //else //{ // alertLogin(); //} } function showDetails(id) { id="div_details_"+id; dialog=art.dialog({ title:'详细信息', drag: false, width:800, resize: false, lock: true, background: '#ccc', // 背景色 opacity: 0.57, // 透明度 content: $("#"+id).html(), }); } function submitComment () { var comment_id = $("#comment_id").val(); var editor_data = CKEDITOR.instances.editor4.getData(); if(editor_data==="") { alert("请输入评论内容"); return; } $.post(baseURL+"/comment", { "type":"comment", "commentID":comment_id, "action":"modify", "content":editor_data, "num":Math.random() }, function(data){ if(data.substring(0,2)=="ok") submitAlert('succeed',data.substring(3)); else submitAlert('error',data); CKEDITOR.instances.editor4.setData(""); setTimeout("refreshThis();",1000); }, "html"); } function modifyComment(obj) { var comment_id=obj.id.replace("modify_","") $("#comment_id").val(comment_id); CKEDITOR.instances.editor4.setData($("#comment_"+comment_id).val()); $("#div_modify_comment").modal(); } $(function(){ $(".table.detailed-table").parent().addClass("tabel-body"); }); </script> <style type="text/css"> .details { display:none; } .jiathis_style .ico{ float: left; font-size: 12px; text-decoration: none; line-height: 18px!important; text-align: left; overflow: hidden; display: block!important; height: 16px!important; line-height: 16px!important; padding-left: 20px!important; cursor: pointer; } .jiathis_style .citeULike{ background: url(/image/bookmarks/citeulike.gif) no-repeat left; } </style> <!--luln20160705--> </div> </div> <div class="row4"> <div id="footer" class="clear"> <div class="footbox"> <ul class="footbox-nav"> <li><a href="/">首页</a></li> <li><a href="/knowledge-analysis?type=researchunit">研究单元产出分布图</a></li> <li><a href="/knowledge-analysis?type=indexed">收录类型分布图</a></li> <li><a href="/knowledge-analysis?type=cited" target="_blank" >论文引用排行</a></li> <li><a href="/browse-author" target="_blank" >作者</a></li> <li><a href="/search-filter?field=dc.type_filter&from=navbar" target="_blank" >文献类型</a></li> <li><a href="/browse-subject" target="_blank" >学科分类</a></li> <li><a href="/help" target="_blank" >使用帮助</a></li> <li><a href="mailto:qinyc@mail.sioc.ac.cn" target="_blank" >联系我们</a></li> </ul> </div> <div style="clear: both;"></div> <div class="site_stat"> <ul> <li>条目量<span class="label label-danger">12237</span></li> <li>全文量<span class="label label-danger">9955</span></li> <li>访问量<span class="label label-danger">1544542</span></li> <li>下载量<span class="label label-danger">243713</span></li> <li> <!--友情链接--> <select onchange="window.location.href=this.value"> <option value="http://www.irgrid.ac.cn">中科院机构知识库网格</option> <option value="http://irsr.llas.ac.cn">综合资源集成登记系统</option> <option value="http://cross.csdl.ac.cn">跨库检索</option> <option value="http://union.csdl.ac.cn/Reader/query.jsp">联合目录</option> <option value="http://sdb.csdl.ac.cn">中国科学文献服务系统</option> <option value="http://dref.csdl.ac.cn">问图书馆员</option> <option value="http://scinews.clas.ac.cn">科技新闻聚合服务</option> <option value="http://www.caswiz.com">中科维智(caswiz)</option> </select> </li> </ul> </div> <div class="footer-copyright col-xs-12">版权所有 @2018 <a href=http://www.sioc.cas.cn>中国科学院上海有机化学研究所</a> - Powered by <a href="http://www.cspace.org.cn/" >CSpace</a></div> <ul class="footer-default"> <li>地址邮编: 中国上海市零陵路345号 (200032)</li>   <!--<li>邮编: </li>  --> <li>电话: 0086-21-54925000</li>   <li></li> <!--<li>备案信息<a id="jgwab" target="_blank" href="http://www.beian.gov.cn/portal/registerSystemInfo?recordcode="></a></li>--> </ul> </a> <!--<div class="address"> <h2><span class="glyphicon glyphicon-envelope"></span> 联系我们</h2> <ul> <li>地址邮编: 中国上海市零陵路345号 (200032)</li> <li>邮编: </li> <li>电话: 0086-21-54925000</li> <li>Email:& <a href="mailto:qinyc@mail.sioc.ac.cn">qinyc@mail.sioc.ac.cn</a></li> </ul> </div>--> </div> </div> </body> </html>