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学科主题: 氟化学
题名: Rational and practical synthesis of alpha,alpha-difluoro-gamma-lactams
其他题名: 合成α,α-二氟-γ-内酯
作者: Li BH(李斌辉) ; Li KL(李可来) ; Chen QY(陈庆云)
通讯作者: 陈庆云
刊名: J. Fluor. Chem.
发表日期: 2012
卷: 133, 页:163-166
收录类别: SCI
部门归属: 中科院上海有机化学研究所; 湖南大学
英文摘要: Treatment of N-phenyl-iododifluoroacetamide (1) with terminal alkenes (2) in the presence of Na2S2O4 and NaHCO3 in CH3CN/H2O gave good yields of N-phenyl-2,2-difluoro-4-iodoalkanamide (3), which cyclized under strong basic conditions to afford N-phenyl-alpha,alpha-difluoro-gamma-lactams (4). Or simply, these lactams 4 can be directly prepared in one-pot from 1 and 2 in the presence of Na2S2O4 and NaOH. (C) 2011 Elsevier B.V. All rights reserved.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000300469500025
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/28309
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Li BH,Li KL,Chen QY. Rational and practical synthesis of alpha,alpha-difluoro-gamma-lactams[J]. J. Fluor. Chem.,2012,133:163-166.
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