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学科主题: 氟化学
题名: 氟烷磺酰氟和全乙酰基保护的吡喃型半缩醛单糖的氟代反应
其他题名: Deoxyfluorination of Peracetylated Pyranose Hemiacetal with Fluoroalkanesulfonyl Fluoride
作者: 严兆华 ; 赖焜民 ; 田伟生 ; 余章昕
通讯作者: 严兆华 ; 田伟生
刊名: 化学学报
发表日期: 2012-01-01
卷: 70, 期:11, 页:1322-1326
收录类别: SCI
部门归属: 南昌大学; 中科院上海有机化学研究所
英文摘要: The deoxyfluorination of peracetylated pyranose hemiacetals with 5-H-3-oxa-1,1,2,2,4,4,5,5-octafluoropentanesulfonyl fluoride (HCF2CF2OCF2CF2SO2F) in the presence of an organic base was investigated resulting in the smooth formation of corresponding glycosyl fluorides in the yield of 44%similar to 94%. The mild reaction conditions and easy work-up procedure are the two advantages for this methodology and it can be used as an alternative method for the preparation of glycosyl fluorides.
语种: 中文
相关网址: 查看原文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/28239
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
严兆华,赖焜民,田伟生,等. 氟烷磺酰氟和全乙酰基保护的吡喃型半缩醛单糖的氟代反应[J]. 化学学报,2012,70(11):1322-1326.
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