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Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers
其他题名Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers
Li ZX(李战雄); DU LIPING; Tang SQ(唐松青); Wang CY(王昌尧)
2009
发表期刊Chin. J. Chem.
ISSN1001-604X
卷号27期号:12页码:2429-2432
摘要Using 3,5 -bis(trifluoromethyl)bromobenzene and methyltrimethoxysilane or tetraethoxysilane as raw materials, novel trifluoromethylphenyl silanes were synthesized via Grignard reaction and substitution reaction, and the molecular structure of silane products was characterized by NMR, FT-IR, MS techniques and elemental analysis. The reaction result showed that the reactivity of Grignard reagent was different in THF and diethyl ether when subjected to substitution reaction, which gave three products with different substitution degree. According to the current work, mono-, di- and tri-substituted product can be obtained selectively from the same reactants by controlling the reaction condition.
学科领域氟化学
部门归属中国科学院上海有机化学研究所; 苏州大学
URL查看原文
收录类别SCI
语种英语
WOS记录号WOS:000273627600022
引用统计
被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/27765
专题上海有机化学研究所
通讯作者Tang SQ(唐松青)
推荐引用方式
GB/T 7714
Li ZX,DU LIPING,Tang SQ,et al. Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers[J]. Chin. J. Chem.,2009,27(12):2429-2432.
APA 李战雄,DU LIPING,唐松青,&王昌尧.(2009).Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers.Chin. J. Chem.,27(12),2429-2432.
MLA 李战雄,et al."Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers".Chin. J. Chem. 27.12(2009):2429-2432.
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