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学科主题: 氟化学
题名: Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers
其他题名: Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers
作者: Li ZX(李战雄) ; DU LIPING ; Tang SQ(唐松青) ; Wang CY(王昌尧)
通讯作者: 唐松青
刊名: Chin. J. Chem.
发表日期: 2009-01-01
卷: 27, 期:12, 页:2429-2432
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所; 苏州大学
英文摘要: Using 3,5 -bis(trifluoromethyl)bromobenzene and methyltrimethoxysilane or tetraethoxysilane as raw materials, novel trifluoromethylphenyl silanes were synthesized via Grignard reaction and substitution reaction, and the molecular structure of silane products was characterized by NMR, FT-IR, MS techniques and elemental analysis. The reaction result showed that the reactivity of Grignard reagent was different in THF and diethyl ether when subjected to substitution reaction, which gave three products with different substitution degree. According to the current work, mono-, di- and tri-substituted product can be obtained selectively from the same reactants by controlling the reaction condition.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000273627600022
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/27765
Appears in Collections:上海有机化学研究所_期刊论文

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Recommended Citation:
Li ZX,DU LIPING,Tang SQ,et al. Synthesis and Characterization of Novel Trifluoromethylphenyl Silane Monomers[J]. Chin. J. Chem.,2009,27(12):2429-2432.
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