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学科主题: 有机化学
题名: N,N'-二(硝基呋咱基)草酰胺合成及性能研究
其他题名: Synthesis and properties of N,N'-Bis(nitrofurazano)oxalamide
作者: 李战雄 ; 欧育湘 ; 陈博仁
刊名: 含能材料
发表日期: 2002-01-01
卷: 10, 期:1, 页:10-12
部门归属: 中国科学院上海有机化学研究所元素有机化学实验室; 北京理工大学化工与材料学院
摘要: 以3,4—二氨基呋咱为原料经酰化合成出 N,N'-二(硝基呋咱基)草酰胺(DNFOA)。利用IR,1~HNMR, MS和元素分析对其结构进行了鉴定。用悬浮法测定 DNFOA密度为1.90g.cm~-3,计算其标准生成焓为303.6kJ. Mol~-1,爆速8 559.6 m. S~-1,爆压33.6 Gpa。DNFOA的撞击感度为82 cm(H^50,5kg8落锤)。
英文摘要: N,N'-di(nitrofurazano) oxalamide (DNFOA) was synthesized from 3,4-diaminofurazan by acidylating. The structrure of DNFOA has been identified by IR, ~1HNMR, MS and elemental analysis. The density of DNFOA was determined to be 1.90g.cm~3 by suspension method. The values of the standard enthalpy, the detonation velocity and the explosive pressure at C-J point were calculated to be 303.6 Kj.mol~1,8 559.6m.s~-1,33.6 Gpa, respectively. As a low-sensitiviety high energetic density compound, the impact-sensitivity (H^50)of DNFOA was mensurated to be 82 cm (5 kg drop hammer).
语种: 中文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/27535
Appears in Collections:上海有机化学研究所_期刊论文

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Recommended Citation:
李战雄,欧育湘,陈博仁. N,N'-二(硝基呋咱基)草酰胺合成及性能研究[J]. 含能材料,2002,10(1):10-12.
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