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学科主题: 天然产物有机化学
题名: A new synthesis of tanikolide
其他题名: Tanikolide 的一种新合成方法
作者: Zhai HB(翟宏斌) ; Chen QS(陈庆寿) ; Zhao JR(赵景瑞) ; Luo SJ(罗盛军) ; Jia XS(贾学顺)
通讯作者: 翟宏斌
刊名: Tetrahedron Lett.
发表日期: 2003
卷: 44, 期:14, 页:2893-2894
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所现代有机化学实验室; 上海大学化学系
英文摘要: We report a concise synthesis of tanikolide 1, which was obtained from ethyl 2-oxocyclopentanecarboxylate in four steps: alkylation, Baeyer-Villiger reaction, saponification, and reduction/lactonization, in 70% overall yield. Our strategy should be suitable for the preparation of 1 in multigram or larger quantities. The net result of the last two steps(i.e. saponification and reduction/lactonization)is an efficient reduction of the ethoxycarbonyl of 3 while keeping the lactone carbonyl intact.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000181893800029
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/25563
Appears in Collections:中科院天然产物有机化学重点实验室_期刊论文

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Recommended Citation:
Zhai HB,Chen QS,Zhao JR,et al. A new synthesis of tanikolide[J]. Tetrahedron Lett.,2003,44(14):2893-2894.
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