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学科主题: 高分子化学
题名: 叶立德活性聚合制备基于聚亚甲基的大分子单体
其他题名: Synthesis of Polymethylene-based Macromonomer by Living Polymerization of Ylides
作者: 赵亮 ; 陈健壮 ; 史丽萍 ; 陈蔚红 ; 李光玉 ; 王玉东 ; 马志
通讯作者: 王玉东 ; 马志
刊名: 化学学报
发表日期: 2011-01-01
卷: 69, 期:5, 页:591-595
收录类别: SCI
部门归属: 郑州大学材料科学与工程学院; 中国科学院上海有机化学研究所
英文摘要: Two kinds of polymethylene-based macromonomers were prepared by living polymerization of ylides. One macromonomer PM-methacrylate was obtained by the transformations of hydroxyl group at the chain end of polymethylene obtained by living polymerization of ylides. The other macromonomer PM-styryl was synthesized via living polymerization of ylides which initiated by organoborane which was prepared by hydroboration of divinylbenzene, and after the oxidation by trimethylamine-N-oxide dehydrate (TAO), alpha-p-vinylphenyl-omega-hydroxypolymethylene were obtained. The chain structure, molecular weight and its distribution of the two macromonomers were investigated by high temperature (1)H NMR spectra, FT-IR and high temperature GPC.
语种: 中文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/25407
Appears in Collections:分析化学研究室_期刊论文

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Recommended Citation:
赵亮,陈健壮,史丽萍,等. 叶立德活性聚合制备基于聚亚甲基的大分子单体[J]. 化学学报,2011,69(5):591-595.
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