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学科主题: 氟化学
题名: One-pot asymmetric synthesis of alpha-trifluoromethylated amines from alpha-trifluoromethyl ketones
其他题名: α-三氟甲基酮一锅法不对称合成α-三氟甲基胺
作者: Xu J(徐剑) ; Liu ZJ(刘振江) ; Yang XJ(杨先金) ; Wang LM(王利民) ; Chen GL(陈冠龙) ; Liu JT(刘金涛)
通讯作者: 杨先金 ; 刘金涛
刊名: Tetrahedron
发表日期: 2010-01-01
卷: 66, 期:46, 页:8933-8937
收录类别: SCI
部门归属: 华东理工大学; 中国科学院上海有机化学研究所
英文摘要: Diastereoselective reduction of (Rs)-N-tert-butanesulfinyl alpha-trifluoromethyl ketimines formed in situ from the corresponding alpha-trifluoromethyl ketones and N-tert-butanesulfinamide has been achieved, and either diastereomer of N-tert-butanesulfinyl alpha-trifluoromethyl amines was obtained in good yields with excellent diastereoselectivities (up to 99:1 dr) using NaBH4 and L-Selectride as the reductants, respectively. (C) 2010 Elsevier Ltd. All rights reserved.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000284499100019
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/23378
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Xu J,Liu ZJ,Yang XJ,et al. One-pot asymmetric synthesis of alpha-trifluoromethylated amines from alpha-trifluoromethyl ketones[J]. Tetrahedron,2010,66(46):8933-8937.
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