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学科主题: 有机化学
题名: 3,4-双(叠氮乙酰胺基)呋咱的合成及其晶体结构
其他题名: Synthesis and crystal structure of 3,4-bis(azidoacetamino)furazan
作者: 李战雄 ; 唐松青 ; 刘金涛
刊名: 结构化学
发表日期: 2003-01-01
卷: 22, 期:1, 页:25-28
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所元素有机化学实验室
英文摘要: 3,4Bis(azidoacetamino)furazan (DAZAF) was synthesized and characterized by elementl analysis, IR, ~1H NMR and MS as an energetic compound. The crystal structure of the title compund was determined by single-crystal X-ray diffraction with the following data: C^6H^6N^10O^3, monocilinic, P21/n, Z=4α=8.402(3), b=15.146(3), c=9.247(3) A,β=111.09(2)°, V=1098.0(6)A,~3, Mr=266.18, Dc=1.610g/cm~3, F(000)=544,μ=1.34cm~-1, R=0.037 and wR=0.044 for 2136 observed reflections (I>2σ(I). Intra-and inter-molecular hydrogen bonds were identified between the O and H atoms of two intramolecular acetylamino groups and two intermolecular acetylamino groups, respectively.
语种: 中文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/23310
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
李战雄,唐松青,刘金涛. 3,4-双(叠氮乙酰胺基)呋咱的合成及其晶体结构[J]. 结构化学,2003,22(1):25-28.
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