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学科主题: 金属有机化学
题名: 4-羟基-3,5-二硝基吡啶氮氧化物铅及铜盐的合成
其他题名: Synthesis of lead(II) and copper(II) salts of 4-hydroxy-3,5-dinitropyridine oxide
作者: 郑玉梅 ; 邓敏智 ; 赵凤起 ; 袁潮
刊名: 火炸药学报
发表日期: 2002-01-01
期: 4, 页:51-52,13
部门归属: 中国科学院上海有机化学研究所金属有机化学开放实验室; 西安近代化学研究所
摘要: 从吡啶出发经过多步反应以较高的产率制得了4—羟基—3,5—二硝基吡啶氮氧化物的铅、铜盐,并通过质谱及元素分析等方法对其进行了结构确定。经DSC及TG的分析表明.该类化合物对RDX、AP及NC十NG等的热分解都具有催化作用,且使其产生出更多的分解热,表现出良好的合能催化剂的特征。
英文摘要: The paper describes that synthesis of lead(II) and copper(II) salts of 4-hydroxy-3,5-dinitropyridine oxide in good yields from pyridine via the multiple steps. The salts were characterized by M>S. and microanalysis. DSC and TG experimental results of the salts showed that the salts could effectively catalyze the thermal decomposition of RDX, AP and NC+NG, Meanwhile, the decomposition heats of mixturescontaining different salts were larger than those of the corresponding pure RDX AP and NC+NG.The all facts suggested the salts might be better energetic burning catalysts.
语种: 中文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/23106
Appears in Collections:金属有机化学国家重点实验室_期刊论文

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Recommended Citation:
郑玉梅,邓敏智,赵凤起,等. 4-羟基-3,5-二硝基吡啶氮氧化物铅及铜盐的合成[J]. 火炸药学报,2002(4):51-52,13.
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