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Novel thermolytic products and their structures derived from thermolysis of isomerized products of spiro[4.4]nona-1,3-diene(dicarbonyl)[ethoxy(aryl) carbene]iron phosphine adducts [(eta(3)-C9H12)Fe{C(OC2H5)Ar}(CO)(2)PPh3]
其他题名Novel thermolytic products and their structures derived from thermolysis of isomerized products of spiro[4.4]nona-1,3-diene(dicarbonyl)[ethoxy(aryl) carbene]iron phosphine adducts [(eta(3)-C9H12)Fe{C(OC2H5)Ar}(CO)(2)PPh3]
Xiao N(肖努); Sun J(孙杰); Zhu HP(朱沪平); 津森展子; Chen JB(陈家碧)
2008
发表期刊Inorg. Chim. Acta
ISSN0020-1693
卷号361期号:11页码:3171-3176
摘要Heating a benzene solution of the isomerized product of spiro[4.4]nona-1,3-diene(dicarbonyl)[ethoxy(aryl)carbene]iron phosphine adduct[(eta(3)-C9H12)Fe{C(OC2H5)(C6H4CH3-o)}(CO)(2)PPh3] (1) in a sealed quartz tube at 85-90 degrees C for 72 h gave the ring-opened eta(4) olefin-coordinated dicarbonyliron phosphine complex [Fe{eta(4)-C5H7CH=CHCH2CH=C(OC2H5)C6H4CH3-o}(CO)(2)PPh3] (3) and cyclobutane derivative [C24H22O7] (4). The thermal decomposition of analogous isomerized product [(eta(3)-C9H12)Fe{C(OC2H5)(C6H4CH3-p)}-(CO)(2)PPh3] (2) afforded the corresponding eta(4) olefin-coordinated dicarbonyliron phosphine complex [Fe{eta(4)-C5H7CH=CHCH2CH=C(OC2H5)C(6)H(4)CH(3-)p}(CO)(2)PPh3] (6) and compound 4. The structures of products 3 and 4 have been established by X- ray diffraction studies. (c) 2007 Elsevier B.V. All rights reserved.
学科领域金属有机化学
部门归属Toyama Natl Coll Technol; 上海有机所
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收录类别SCI
语种英语
文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/21425
专题金属有机化学国家重点实验室
通讯作者Chen JB(陈家碧)
推荐引用方式
GB/T 7714
Xiao N,Sun J,Zhu HP,et al. Novel thermolytic products and their structures derived from thermolysis of isomerized products of spiro[4.4]nona-1,3-diene(dicarbonyl)[ethoxy(aryl) carbene]iron phosphine adducts [(eta(3)-C9H12)Fe{C(OC2H5)Ar}(CO)(2)PPh3][J]. Inorg. Chim. Acta,2008,361(11):3171-3176.
APA 肖努,孙杰,朱沪平,津森展子,&陈家碧.(2008).Novel thermolytic products and their structures derived from thermolysis of isomerized products of spiro[4.4]nona-1,3-diene(dicarbonyl)[ethoxy(aryl) carbene]iron phosphine adducts [(eta(3)-C9H12)Fe{C(OC2H5)Ar}(CO)(2)PPh3].Inorg. Chim. Acta,361(11),3171-3176.
MLA 肖努,et al."Novel thermolytic products and their structures derived from thermolysis of isomerized products of spiro[4.4]nona-1,3-diene(dicarbonyl)[ethoxy(aryl) carbene]iron phosphine adducts [(eta(3)-C9H12)Fe{C(OC2H5)Ar}(CO)(2)PPh3]".Inorg. Chim. Acta 361.11(2008):3171-3176.
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