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学科主题: 有机化学
题名: Facile cleavage of triethylsilyl (TES) ethers using o-lodoxybenzoic acid (IBX) without affecting tert-butyldimethylsilyl(TBS)ethers
其他题名: 使用邻碘氧苯甲酸高效裂解三乙基硅醚(TES)而又不影响二甲基叔丁基硅醚的方法
作者: Wu YK(伍贻康) ; Huang JH(黄嘉慧) ; Shen X(沈鑫) ; Hu Q(胡祺) ; Tang CJ(唐朝军) ; Li L(李亮)
通讯作者: 伍贻康
刊名: Org. Lett.
发表日期: 2002-01-01
卷: 4, 期:13, 页:2141-2144
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所生命有机化学实验室
英文摘要: In DMSO cleavage of triethylsilyl (TES) ethers by o-iodoxybenzoic acid (IBX) was significantly faster than cleavage of tert-butyldimethylsilyl (BS) ethers or further oxidation into carbonyl compounds. In most cases, TES protecting groups could be removed in good to excellent yields within 1 h, whereas similar TBS protecting groups remained intact under the same conditions. The procedure also could be adapted for direct one-pot conversion of TES ethers into carbonyl compounds.
语种: 英语
相关网址: 查看原文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/20313
Appears in Collections:生命有机化学国家重点实验室_期刊论文

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Recommended Citation:
Wu YK,Huang JH,Shen X,et al. Facile cleavage of triethylsilyl (TES) ethers using o-lodoxybenzoic acid (IBX) without affecting tert-butyldimethylsilyl(TBS)ethers[J]. Org. Lett.,2002,4(13):2141-2144.
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