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学科主题: 天然产物有机化学
题名: A convenient synthesis of N-fluorenylmethoxycarbonyl-N-methyl-L-cysteine derivatives[Fmoc,Ce-Cys(R)-OH]
其他题名: 一种方便的合成N-芴甲氧碳基-N-甲基-L-巯基丙氨酸衍生物的合成 [Fmoc,Ce-Cys(R)-OH]
作者: Liu JF(刘家峰) ; Tang XX(汤晓霞) ; Jiang B(姜标)
通讯作者: 姜标
刊名: Synthesis
发表日期: 2002-01-01
期: 11, 页:1499-1501
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所金属有机化学开放实验室
英文摘要: The synthesis of N-fluorenylmethoxycarbonyl-N-S-dimethyl-L-Cysiteine (1) [Fmoc, Me-Cys(Me)-OH] and N-fluorenylmcthoxycarbonyl-N-methyl-S-acetamidomethyl-L-Cysteine (2) [Fmoc.Me-Cys(Acm)-OH] is reported. The synthesis is characterized by a convenient two-step procedure from ?-thiazolidine-4-carboxylic acid (3) via reduction and subsequent protection. Crystals of 1, which have been analyzed by single-crystal X-ray crystal lography, are obtained after a simple crystallization at the end of the process, without purification of intermediates.
语种: 英语
相关网址: 查看原文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/20153
Appears in Collections:中科院天然产物有机化学重点实验室_期刊论文

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Recommended Citation:
Liu JF,Tang XX,Jiang B. A convenient synthesis of N-fluorenylmethoxycarbonyl-N-methyl-L-cysteine derivatives[Fmoc,Ce-Cys(R)-OH][J]. Synthesis,2002(11):1499-1501.
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