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学科主题: 分析化学
题名: Analysis of Volatile Compounds in Radix Bupleuri Injection by GC-MS-MS
其他题名: GC-MS-MS分析柴胡注射液中的挥发性成分
作者: Liu SH(刘素红) ; Lu SS(陆森森) ; Su Y(苏越) ; Guo YL(郭寅龙)
通讯作者: 苏越 ; 郭寅龙
刊名: Chromatographia
发表日期: 2011
卷: 74, 期:5-6, 页:497-502
收录类别: SCI
部门归属: 上海中医药大学; 中科院上海有机化学研究所
英文摘要: Static headspace sampling, headspace solid-phase microextraction, and direct immersion solid-phase microextraction coupled with gas chromatography-tandem mass spectrometry have been developed for determination of the volatile components in Radix bupleuri injection. A total of 78 compounds were identified from Radix bupleuri injection. Direct immersion solid-phase microextraction gave a better extraction efficiency for polar compounds, including organic acids and alcohols, than headspace solid-phase microextraction or static headspace sampling. Product ion isotope pattern analysis was applied to determine the elemental composition of the precursor ion, which could make the qualitative analysis more accurate and reliable.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000294066000021
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/20046
Appears in Collections:分析化学研究室_期刊论文

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Recommended Citation:
Liu SH,Lu SS,Su Y,et al. Analysis of Volatile Compounds in Radix Bupleuri Injection by GC-MS-MS[J]. Chromatographia,2011,74(5-6):497-502.
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