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学科主题: 氟化学
题名: Synthesis of herbicidal ZJ0273 labeled with tritium and carbon-14
其他题名: Synthesis of herbicidal ZJ0273 labeled with tritium and carbon-14
作者: Yang ZM(杨征敏) ; Ye QF(叶庆富) ; Lv L(吕龙)
通讯作者: 叶庆富 ; 吕龙
刊名: J. Label. Compd. Radiopharm.
发表日期: 2008-01-01
卷: 51, 期:3-4, 页:182-186
收录类别: SCI
部门归属: 上海有机所; 西北大学; 浙江大学
英文摘要: ZJ0273, propyl 4-(2-(4,6-dimethoxypyrimidin-2-yloxy)benzylamino)benzoate, is a broad-spectrum herbicidal ingredient used for weed control in oilseed rape in China. Two mono-labeled ZJ0273, propyl 4-(2-(4,6-dimethoxypyrimidin-2-yloxy)[phenyl-3,4,5,6-H-3(4)]benzylamino) benzoate (7) and propyl 4-(2-(4,6-dimethoxy[4,6-C-14(2)]pyrimidin-2-yloxy)benzylamino)benzoate (12), were synthesized separately from [2,3,4,5,6-H-3(5)]phenol in a four-step yield of 27% and from 4,6-dichloro-2-(methylthio)[4,6-C-14(2)]pyrimidine in a three-step yield of 54%. in addition, two dual-labeled analogues of ZJ0273 were prepared by homogeneously mixing tritium-labeled ZJ0273 (7) in the benzyl ring separately with two carbon-14-labeled ZJ0273 (2, 12) in the benzoate ring and the pyrimidine ring. These labeled ZJ0273 could be used as radiotracers in the studies on the metabolism, mode of action, environmental behavior, and fate of ZJ0273.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000255730400010
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/19199
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Yang ZM,Ye QF,Lv L. Synthesis of herbicidal ZJ0273 labeled with tritium and carbon-14[J]. J. Label. Compd. Radiopharm.,2008,51(3-4):182-186.
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