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学科主题: 氟化学
题名: Design and synthesis of novel perfluoroalkyl-containing zinc pyrithione biocide
其他题名: 设计与合成一类新型的含全氟烷基的Zinc Pyrithione
作者: Sun JY(孙建英) ; Qiu XL(邱小龙) ; Meng WD(孟卫东) ; Qing FL(卿凤翎)
通讯作者: 卿凤翎
刊名: Tetrahedron
发表日期: 2006
卷: 62, 期:37, 页:8702-8706
收录类别: SCI
部门归属: 东华大学; 中科院上海有机化学研究所
英文摘要: Novel perfluoroalkyl-containing zinc pyrithione biocide 2 was designed and synthesized in six steps. Reaction of 4-methylpyridine with C8F17(CH2)(3)I in the presence of LDA followed by further oxidization of the resultant pyridine derivative 6 gave the pyridine N-oxide 9. Treatment of 9 with phosphorous oxychloride afforded the desirable chloride 12. Oxidization of compound 12 with H2O2 gave N-oxide 14, which was treated with NaSH to give the sulfide 3. Finally, treatment of compound 3 with NaOH/ZnSO4 smoothly delivered perfluoroalkyl-containing zinc pyrithione biocide 2 in good yield. (c) 2006 Elsevier Ltd. All rights reserved.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000240125800005
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/17573
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Sun JY,Qiu XL,Meng WD,et al. Design and synthesis of novel perfluoroalkyl-containing zinc pyrithione biocide[J]. Tetrahedron,2006,62(37):8702-8706.
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