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Synthesis and characterization of novel fluoropolymers containing sulfonyl and perfluorocyclobutyl units
其他题名新型的含砜基和全氟环丁基氟聚合物的合成与表征
Huang XY(黄晓宇); Wang RW(王若文); Zhao PQ(赵品桥); Chen GD(陈国栋); Zhang S(张森); Qing FL(卿凤翎)
2005
发表期刊Polymer
ISSN0032-3861
卷号46期号:18页码:7590-7597
摘要A novel sulfonyl-containing monomer, 4,4'-sulfonyl-bis(trifluorovinyloxy)biphenyl, and the resulting fluoropolymers with good thermal stability have been prepared. The monomer was synthesized by two steps using 4,4'-sulfonyldiphenol as starting material and characterized by FT-IR, H-1 NMR, C-13 NMR. F-19 NMR and element analysis in detail. Fluoropolymers containing sulfonyl and perfluorocyclobutyl units were prepared by different polymerization methods. A series Of fluoropolymers with higher molecular weights were obtained by solution polymerization in diphenyl ether. The molecular weight is dependent on the polymerization time, polymerization temperature and the concentration of the monomer. The resulting polymers show excellent Solubility in conventional solvents and good thermal stability with a high decomposition temperature about 500 degrees C measured by TGA. (c) 2005 Elsevier Ltd. All rights reserved.
学科领域氟化学
部门归属上海有机所; 东华大学
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收录类别SCI
语种英语
WOS记录号WOS:000231397200088
引用统计
被引频次:17[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/17533
专题中科院有机氟化学重点实验室
通讯作者Huang XY(黄晓宇); Qing FL(卿凤翎)
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GB/T 7714
Huang XY,Wang RW,Zhao PQ,et al. Synthesis and characterization of novel fluoropolymers containing sulfonyl and perfluorocyclobutyl units[J]. Polymer,2005,46(18):7590-7597.
APA 黄晓宇,王若文,赵品桥,陈国栋,张森,&卿凤翎.(2005).Synthesis and characterization of novel fluoropolymers containing sulfonyl and perfluorocyclobutyl units.Polymer,46(18),7590-7597.
MLA 黄晓宇,et al."Synthesis and characterization of novel fluoropolymers containing sulfonyl and perfluorocyclobutyl units".Polymer 46.18(2005):7590-7597.
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