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学科主题: 有机化学
题名: Synthesis of heteroarylazo-substituted calix[4]arenes
其他题名: 杂芳环偶氮取代杯芳烃-4合成
作者: Jin CM(金传明) ; Lu GY(陆国圆) ; Zhen-Sheng Wang ; Xiao- Zeng You ; Wang ZH(王中华) ; Gong W(龚炜) ; Wu HM(吴厚铭)
通讯作者: 陆国圆
刊名: Synthesis
发表日期: 2001
期: 7, 页:1023-1026
收录类别: SCI
部门归属: 南京大学; 中国科学院上海有机化学研究所生命有机国家开放实验室
英文摘要: This paper reports a novel method for preparing heteroarylazo- subsituted calix[4]arenes, in which heteroaromatic amines were diazotized with isoamyl nitrite in EtON^a-EtOH under refluxing conditions. Mono(heteroarylazo)-, bis(heteroarylazo)-and tetrakis(heteroarylazo)-substituted calix[4]arenes were obtained as main product by diazo-coupling in differen molar ratio to calix[4]arenes under pH8-9 in non-aqueous solution at 0-5℃. Based on the method, eight novel heteoarylazo-substituted calix[4]arenes have been synthesized by diao-coupling reaction ofcalix[4]arene with diazonium salt solutions of 4-aminopyridine or 2-aminothiazole.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000169397600008
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/17283
Appears in Collections:上海有机化学研究所_期刊论文

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Recommended Citation:
Jin CM,Lu GY,Zhen-Sheng Wang,et al. Synthesis of heteroarylazo-substituted calix[4]arenes[J]. Synthesis,2001(7):1023-1026.
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