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学科主题: 有机化学
题名: A practical high through-put continuous process for the synthesis of chiral cyanohydrins
其他题名: 一个合成手性氰腈醇的有效的高通量的流动相装置的设计
作者: Chen PR(陈沛然) ; Han SQ(韩世清) ; Lin GQ(林国强) ; Li ZY(李祖义)
通讯作者: 林国强
刊名: J. Org. Chem.
发表日期: 2002
卷: 67, 期:23, 页:8251-8253
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所现代有机合成化学实验室
英文摘要: A practical high through-put continuous processfor the synthesis of chiral cyanohydrins is reported. Pretreated almond meal (or other solid raw enzyme sources) was loaded in a column to form a reactor, to which were attached a supplying system to deliver a solution of substrate and HCN in solvent on one end and a collecting-separating system on the other end. Bycontrolling the flowing rate, optimal conditions were achieved for the hydrocyanation of various aromatic carboxaldehydes in a "micro-aqueous”medium to produce chiral cyanohydrins in high yields and high enantiomeric excess (ee) with high substrate/catalyst ratio.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000179110400045
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/16607
Appears in Collections:中科院天然产物有机化学重点实验室_期刊论文

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Recommended Citation:
Chen PR,Han SQ,Lin GQ,et al. A practical high through-put continuous process for the synthesis of chiral cyanohydrins[J]. J. Org. Chem.,2002,67(23):8251-8253.
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