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学科主题: 有机氟化学
题名: Unexpected formation of N-fluoroalkaneacyl anilides from the reactions of fluoroalkanesulfonyl azides with nitrobenzene and its derivatives
其他题名: 氟烷基磺酰叠氮与硝基苯及其衍生物反应意外的生成N-氟烷基酰基苯胺类化合物
作者: Xiong WT(熊婉婷) ; Zhao JW(赵经纬) ; Gu JW(顾继伟) ; Zhu SZ(朱仕正)
通讯作者: 朱仕正
刊名: Tetrahedron
发表日期: 2011
卷: 67, 期:29, 页:5235-5243
收录类别: SCI
部门归属: 中科院上海有机化学研究所
英文摘要: The thermal reactions of fluoroalkanesulfonyl azides R(f)CF(2)SO(2)N(3) 1 with nitrobenzene and its derivatives XC(6)H(4)NO(2) (X=H, F, Cl, CF(3)) gave the unexpected N-fluoroalkaneacyl anilides R(f)CONHC(6)H(4)X (X=H, Cl, F, CF3) in addition to fluoroalkanesulfonyl amides R(f)CF(2)SO(2)NH(2). Under the same reaction conditions, however, nitrobenzene containing an electron-donating group RC(6)H(4)NO(2) (R=CH(3), OCH(3)) reacted with 1 affording the corresponding N-fluoroalkanesulfonyl anilides R(f)CF(2)SO(2)NHC(6)H(3)(NO(2))R. Other electron-poor benzene derivatives, such as benzaldehyde, benzoate, and acetophenone C(6)H(5)Y(Y=CHO, COCH(3), CO(2)CH(3)) all gave the meta-substituted N-fluoroalkanesulfonyl anilides R(f)CF(2)SO(2)NHC(6)H(4)Y. (C) 2011 Elsevier Ltd. All rights reserved.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000292472300015
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/14520
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Xiong WT,Zhao JW,Gu JW,et al. Unexpected formation of N-fluoroalkaneacyl anilides from the reactions of fluoroalkanesulfonyl azides with nitrobenzene and its derivatives[J]. Tetrahedron,2011,67(29):5235-5243.
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