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学科主题: 有机氟化学
题名: Crystal structure of a supramolecular complex formed between 1-bromo-2-iodo-tetrafluoroethane and N,N,N ',N '-tetramethyl-ethylenediamine '-tetramethyl-ethylenediamine; supramolecular complex
其他题名: 1-溴-2-碘四氟乙烷和N,N,N’,N’-四亚甲基二胺形成的超分子混合物的晶体结构
作者: Huang QC(黄其辰) ; Wang ZM(王哲明) ; Chu QL(储千里) ; Zhu SZ(朱仕正)
通讯作者: 黄其辰
刊名: J. Incl. Phenom. Macrocycl. Chem.
发表日期: 2006-01-01
卷: 54, 期:3-4, 页:177-180
收录类别: SCI
部门归属: 北京大学; 中科院上海有机化学研究所
英文摘要: X-ray analysis has revealed that N,N,N',N'-tetramethyl-ethylenediamine 1 form donor-acceptor complex 3 with 1-bromo-2-iodo-tetrafluoroethane 2, in which the N X (X = Br, 1) distances are longer than the average covalent bond length between X and N, but are also definitively shorter than the sum of the corresponding van der Waals radii of X and N, thus that indicating weak interactions between the nitrogen and bromine or iodine atoms. In our experimental section, a valuable method for recrystallization and collect X-ray data from crystals that easily exhibit decay and can be cracked is reported.
语种: 英语
相关网址: 查看原文
内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/14390
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Huang QC,Wang ZM,Chu QL,et al. Crystal structure of a supramolecular complex formed between 1-bromo-2-iodo-tetrafluoroethane and N,N,N ',N '-tetramethyl-ethylenediamine '-tetramethyl-ethylenediamine; supramolecular complex[J]. J. Incl. Phenom. Macrocycl. Chem.,2006,54(3-4):177-180.
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