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学科主题: 有机氟化学
题名: Reactions of fluoroalkanesulfonyl azides with trimethylsilyl enol ethers
其他题名: 氟烷砜基叠氮与三甲基烯醇硅醚的反应研究
作者: Xu Y(许勇) ; Xu GL(许国林) ; Zhu SZ(朱仕正) ; Zhu GY(朱光宇) ; Jia YS(贾一四) ; Huang QC(黄其辰)
通讯作者: 朱仕正
刊名: J. Fluor. Chem.
发表日期: 1999
卷: 96, 页:79-85
收录类别: SCI
部门归属: 中国科学院上海有机化学研究所有机氟化学开放实验室; 北京大学
英文摘要: Reactions of per(poly)-fluoroalkanesulfonyl azides R=fSO=2N=3 with trimethylsily enol ethers RCH=C(H)OSiMe=3 (R=1=tBu, Ph)afforded α-[N-(fluoroalkanesulfonyl)] amino ketones RC(O)CH=2NHSO=2R=f in good yields. The cycloanalog 1-cyclohexenyl trimethylsilyl ether reacted with the azides to give one-carbon ring-contracted product N-fluoroalkanesulfonyl cyclopentanecarboxamides, c -C=5H=11CONH-SO=2R=f. In the case of 1-cyclooctenyl trimethylsilyl ether, however, two products α-[N-(fluoroalkane sulfonyl)amine cyclooctanones and c-C=7H=13CONHSO=2R=f were obtained.
语种: 英语
相关网址: 查看原文
WOS记录号: WOS:000081013400016
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内容类型: 期刊论文
URI标识: http://ir.sioc.ac.cn/handle/331003/14216
Appears in Collections:中科院有机氟化学重点实验室_期刊论文

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Recommended Citation:
Xu Y,Xu GL,Zhu SZ,et al. Reactions of fluoroalkanesulfonyl azides with trimethylsilyl enol ethers[J]. J. Fluor. Chem.,1999,96:79-85.
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