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Hydrogen-bonded aryl amide macrocycles: Synthesis, single-crystal structures, and stacking interactions with fullerenes and coronene
其他题名氢键介质的芳酰胺大环: 合成、晶体结构和与富勒烯的芳香作用
Zhu YY(朱元元); Li C(李闯); Li GY(李光玉); Jiang XK(蒋锡夔); Li ZT(黎占亭)
2008
发表期刊J. Org. Chem.
ISSN0022-3263
卷号73期号:5页码:1745-1751
摘要[Graphics] Six hydrogen-bonded shape-persistent aryl amide macrocycles have been prepared by using one-step and (for some) step-by-step approaches. From the one-step reactions, 3 + 3, 2 + 2, or even 1 + 1 macrocycles were obtained in modest to good yields. The reaction selectivity was highly dependent on the structures of the precursors. The X-ray structural analysis of two methoxyl-bearing macrocycles revealed intramolecular hydrogen bonding and weak intermolecular stacking interaction; no column-styled stacking structures were observed. The H-1 (DOSY) NMR, UV-vis, and fluorescent experiments indicated that the new rigidified macrocycles complex fullerenes or coronene in chloroform through intermolecular,pi-stacking interaction. The association constants of the corresponding 1: 1 complexes have been determined if the stacking was able to cause important fluorescent quenching of the macrocycles or coronene.
学科领域物理有机化学
部门归属上海有机所
URL查看原文
收录类别SCI
语种英语
WOS记录号WOS:000253595100009
引用统计
被引频次:70[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.sioc.ac.cn/handle/331003/12718
专题物理有机化学研究室
通讯作者Li ZT(黎占亭)
推荐引用方式
GB/T 7714
Zhu YY,Li C,Li GY,et al. Hydrogen-bonded aryl amide macrocycles: Synthesis, single-crystal structures, and stacking interactions with fullerenes and coronene[J]. J. Org. Chem.,2008,73(5):1745-1751.
APA 朱元元,李闯,李光玉,蒋锡夔,&黎占亭.(2008).Hydrogen-bonded aryl amide macrocycles: Synthesis, single-crystal structures, and stacking interactions with fullerenes and coronene.J. Org. Chem.,73(5),1745-1751.
MLA 朱元元,et al."Hydrogen-bonded aryl amide macrocycles: Synthesis, single-crystal structures, and stacking interactions with fullerenes and coronene".J. Org. Chem. 73.5(2008):1745-1751.
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